Abstract | OBJECTIVES: METHODS: Bovine dentin were prepared with 180-grit paper, conditioned with 0.5M EDTA (pH 7.4) for 60s followed by water rinsing and then blot drying. Each surface was then primed with Phenyl-P/30 wt% HEMA in acetone for 10s followed by blot drying. A light-cured bonding agent was then applied, cured and trimmed to give dumbbell-shaped specimens. The Phenyl-P concentration ranged from 1 to 20 wt%. During the bonding procedure, no compressed air was used. After storage in water at 37 degrees C for one day, tensile bond strengths were measured and analyzed using one-way ANOVA. Dentin discs treated under the same conditions were observed under a scanning electron microscope (SEM). RESULTS: When the concentration of Phenyl-P was 12 wt%, the highest mean tensile bond strength was obtained (27 MPa). It was significantly higher than that of the 3, 5, 15 or 20 wt% groups (9-11 MPa) (p<0.05). The samples of 1 wt% group were all broken during trimming the dumbbell-shaped specimens. SEM observations showed a 1 microm-thick layer of hybridized dentin after polished cross-sections were chemically challenged with 6N HCl for 30s and then 1% NaOCl for 60 min. SIGNIFICANCE: The experimental Phenyl-P/ HEMA acetone primer is effective in bonding resin to EDTA-conditioned dentin. Acetone as a solvent for Phenyl-P/ HEMA primer has the clinical advantage of not requiring an air-stream to evaporate the solvent. The experimental bonding procedure can minimize the skin irritation by HEMA.
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Authors | K Miyasaka, N Nakabayashi |
Journal | Dental materials : official publication of the Academy of Dental Materials
(Dent Mater)
Vol. 17
Issue 6
Pg. 499-503
(Nov 2001)
ISSN: 0109-5641 [Print] England |
PMID | 11567687
(Publication Type: Journal Article, Research Support, Non-U.S. Gov't)
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Chemical References |
- 2-methacryloyloxyethyl phenyl phosphoric acid
- Dentin-Bonding Agents
- Methacrylates
- Organophosphorus Compounds
- Acetone
- hydroxyethyl methacrylate
- Edetic Acid
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Topics |
- Acetone
(chemistry)
- Acid Etching, Dental
- Analysis of Variance
- Animals
- Cattle
- Dental Bonding
- Dentin
(drug effects)
- Dentin Permeability
- Dentin-Bonding Agents
(chemistry)
- Edetic Acid
(chemistry, pharmacology)
- Materials Testing
- Methacrylates
(chemistry)
- Microscopy, Electron, Scanning
- Organophosphorus Compounds
(chemistry)
- Smear Layer
- Surface Properties
- Tensile Strength
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